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Provide clean (and unfrozen) water daily.
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Provide sufficient food (each animal has different diet requirements).
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Keep the living area clean.
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Provide proper grooming (each animal has different needs)
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Provide exercise or the opportunity for the animal to just get out and run.
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If animals are herd animals (such as alpacas), be sure to have at least two.
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Interact with your animals regularly not only so they get used to your being in the pen but also so bonds can form.